Acetal and ketal deprotection using Montmorillonite K10: The first synthesis of syn-4,8-dioxatricyclo[5.1.0.03,5]-2,6-octanedione

Elisabeth C.L. Gautier; Andrew E. Graham; Alexander McKillop; Stephen P. Standen; Richard J K Taylor

doi:10.1016/S0040-4039(97)00226-8

Acetal and ketal deprotection using Montmorillonite K10: The first synthesis of syn-4,8-dioxatricyclo[5.1.0.0^3,5]-2,6-octanedione

Elisabeth C.L. Gautier, Andrew E. Graham, Alexander McKillop, Stephen P. Standen, Richard J K Taylor

Faculty of Computing, Engineering and Science

Research output: Contribution to journal › Article › peer-review

68 Citations (Scopus)

Abstract

Montmorillonite K10 in dichloromethane at room temperature conveniently and efficiently converts acetals and ketals into the corresponding carbonyl compounds. The title dione (diepoxy-1,4- cyclohexanedione) has been prepared for the brat lime using this procedure.

Original language	English
Pages (from-to)	1881-1884
Number of pages	4
Journal	Tetrahedron Letters
Volume	38
Issue number	11
DOIs	https://doi.org/10.1016/S0040-4039(97)00226-8
Publication status	Published - 17 Mar 1997

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title = "Acetal and ketal deprotection using Montmorillonite K10: The first synthesis of syn-4,8-dioxatricyclo[5.1.0.03,5]-2,6-octanedione",

abstract = "Montmorillonite K10 in dichloromethane at room temperature conveniently and efficiently converts acetals and ketals into the corresponding carbonyl compounds. The title dione (diepoxy-1,4- cyclohexanedione) has been prepared for the brat lime using this procedure.",

author = "Gautier, {Elisabeth C.L.} and Graham, {Andrew E.} and Alexander McKillop and Standen, {Stephen P.} and Taylor, {Richard J K}",

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T2 - The first synthesis of syn-4,8-dioxatricyclo[5.1.0.03,5]-2,6-octanedione

AU - Gautier, Elisabeth C.L.

AU - Graham, Andrew E.

AU - McKillop, Alexander

AU - Standen, Stephen P.

AU - Taylor, Richard J K

PY - 1997/3/17

Y1 - 1997/3/17

N2 - Montmorillonite K10 in dichloromethane at room temperature conveniently and efficiently converts acetals and ketals into the corresponding carbonyl compounds. The title dione (diepoxy-1,4- cyclohexanedione) has been prepared for the brat lime using this procedure.

AB - Montmorillonite K10 in dichloromethane at room temperature conveniently and efficiently converts acetals and ketals into the corresponding carbonyl compounds. The title dione (diepoxy-1,4- cyclohexanedione) has been prepared for the brat lime using this procedure.

U2 - 10.1016/S0040-4039(97)00226-8

DO - 10.1016/S0040-4039(97)00226-8

M3 - Article

AN - SCOPUS:0031575828

SN - 1873-3581

VL - 38

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JO - Tetrahedron Letters

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IS - 11

ER -

Acetal and ketal deprotection using Montmorillonite K10: The first synthesis of syn-4,8-dioxatricyclo[5.1.0.03,5]-2,6-octanedione

Abstract

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Acetal and ketal deprotection using Montmorillonite K10: The first synthesis of syn-4,8-dioxatricyclo[5.1.0.0^3,5]-2,6-octanedione