A simple and convenient catalytic procedure for the preparation of dithioacetals

Andrew E. Graham

doi:10.1080/00397919908085819

A simple and convenient catalytic procedure for the preparation of dithioacetals

Andrew E. Graham^*

^*Corresponding author for this work

Faculty of Computing, Engineering and Science

Research output: Contribution to journal › Article › peer-review

6 Citations (Scopus)

Abstract

A simple procedure for the synthesis of cyclic and acyclic thioacetals from aldehydes is described which employs hydrogen chloride solutions generated from acetyl chloride and methanol. It was observed that the reaction could be carded out using catalytic quantities of acetyl chloride, potentially allowing acid sensitive substrates to be used under these conditions.

Original language	English
Pages (from-to)	697-703
Number of pages	7
Journal	Synthetic Communications
Volume	29
Issue number	4
DOIs	https://doi.org/10.1080/00397919908085819
Publication status	Published - 1999

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title = "A simple and convenient catalytic procedure for the preparation of dithioacetals",

abstract = "A simple procedure for the synthesis of cyclic and acyclic thioacetals from aldehydes is described which employs hydrogen chloride solutions generated from acetyl chloride and methanol. It was observed that the reaction could be carded out using catalytic quantities of acetyl chloride, potentially allowing acid sensitive substrates to be used under these conditions.",

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AU - Graham, Andrew E.

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AB - A simple procedure for the synthesis of cyclic and acyclic thioacetals from aldehydes is described which employs hydrogen chloride solutions generated from acetyl chloride and methanol. It was observed that the reaction could be carded out using catalytic quantities of acetyl chloride, potentially allowing acid sensitive substrates to be used under these conditions.

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DO - 10.1080/00397919908085819

M3 - Article

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SN - 0039-7911

VL - 29

SP - 697

EP - 703

JO - Synthetic Communications

JF - Synthetic Communications

IS - 4

ER -

A simple and convenient catalytic procedure for the preparation of dithioacetals

Abstract

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