Barium manganate in microwave-assisted oxidation reactions: synthesis of lactones by oxidative cyclization of diols

Mark C. Bagley; Zhifan Lin; David J. Phillips; Andrew E. Graham

doi:10.1016/j.tetlet.2009.09.117

Barium manganate in microwave-assisted oxidation reactions: synthesis of lactones by oxidative cyclization of diols

Mark C. Bagley^*, Zhifan Lin, David J. Phillips, Andrew E. Graham

^*Awdur cyfatebol y gwaith hwn

Cyfadran Cyfrifiadureg, Peirianneg a Gwyddoniaeth

Allbwn ymchwil: Cyfraniad at gyfnodolyn › Erthygl › adolygiad gan gymheiriaid

22 Dyfyniadau (Scopus)

Crynodeb

Microwave irradiation of a range of diols at 150 °C in acetonitrile in the presence of three equivalents of barium manganate facilitates a novel tandem oxidation/heterocyclocondensation to give the corresponding lactone, including both small and medium ring lactones, in only one hour and in high yield without the need for chromatographic purification.

Iaith wreiddiol	Saesneg
Tudalennau (o-i)	6823-6825
Nifer y tudalennau	3
Cyfnodolyn	Tetrahedron Letters
Cyfrol	50
Rhif cyhoeddi	49
Dynodwyr Gwrthrych Digidol (DOIs)	https://doi.org/10.1016/j.tetlet.2009.09.117
Statws	Cyhoeddwyd - 9 Rhag 2009

Mynediad at Ddogfen

10.1016/j.tetlet.2009.09.117

22 Dyfyniadau
1 Thesis Doethurol

Application of Tandem Oxidation Processes to the Synthesis of Novel Oxabicycloalkane Protein Phosphatase Inhibitors
Phillips, D., 2007
Allbwn ymchwil: Mathau o Thesis › Thesis Doethurol

Dyfynnu hyn

@article{ada06d6f08884f12b5f6b4102774fb5f,

title = "Barium manganate in microwave-assisted oxidation reactions: synthesis of lactones by oxidative cyclization of diols",

abstract = "Microwave irradiation of a range of diols at 150 °C in acetonitrile in the presence of three equivalents of barium manganate facilitates a novel tandem oxidation/heterocyclocondensation to give the corresponding lactone, including both small and medium ring lactones, in only one hour and in high yield without the need for chromatographic purification.",

author = "Bagley, {Mark C.} and Zhifan Lin and Phillips, {David J.} and Graham, {Andrew E.}",

year = "2009",

month = dec,

day = "9",

doi = "10.1016/j.tetlet.2009.09.117",

language = "English",

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pages = "6823--6825",

journal = "Tetrahedron Letters",

issn = "1873-3581",

publisher = "Elsevier",

number = "49",

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TY - JOUR

T1 - Barium manganate in microwave-assisted oxidation reactions

T2 - synthesis of lactones by oxidative cyclization of diols

AU - Bagley, Mark C.

AU - Lin, Zhifan

AU - Phillips, David J.

AU - Graham, Andrew E.

PY - 2009/12/9

Y1 - 2009/12/9

N2 - Microwave irradiation of a range of diols at 150 °C in acetonitrile in the presence of three equivalents of barium manganate facilitates a novel tandem oxidation/heterocyclocondensation to give the corresponding lactone, including both small and medium ring lactones, in only one hour and in high yield without the need for chromatographic purification.

AB - Microwave irradiation of a range of diols at 150 °C in acetonitrile in the presence of three equivalents of barium manganate facilitates a novel tandem oxidation/heterocyclocondensation to give the corresponding lactone, including both small and medium ring lactones, in only one hour and in high yield without the need for chromatographic purification.

U2 - 10.1016/j.tetlet.2009.09.117

DO - 10.1016/j.tetlet.2009.09.117

M3 - Article

AN - SCOPUS:70350007181

SN - 1873-3581

VL - 50

SP - 6823

EP - 6825

JO - Tetrahedron Letters

JF - Tetrahedron Letters

IS - 49

ER -

Barium manganate in microwave-assisted oxidation reactions: synthesis of lactones by oxidative cyclization of diols

Crynodeb

Mynediad at Ddogfen

Ôl bys

Allbwn Ymchwil

Application of Tandem Oxidation Processes to the Synthesis of Novel Oxabicycloalkane Protein Phosphatase Inhibitors

Dyfynnu hyn